Division VI · Laboratory and material analysis Abteilung VI — Labor und Materialanalyse
The division was established in 1974 and is the reason for the word Laboratory in the Institute's name. Its starting point was simple: a date cannot be settled by eye alone, and where two inks or two papers look alike the eye gives up. One person is in post since the second laboratory post fell vacant in July 2025, in the instrument room (EG-1) and the balance room (EG-2) on the ground floor of the laboratory building, sharing the de-ionised water and the extractor bench with the repair workshop next door. The de-ionised water plant and the two rooms that need two people to work in them are the division's chief difficulty, and are described under section 3. The division works first for the Institute's own projects, then for partner institutions and public museums. It does not authenticate objects for private owners and does not value them.
1. What the division works on
- Metal composition and striking practice
- Portable X-ray fluorescence is used to measure the elements present in coins and in seal matrices, so that the recipe of a mint can be followed over time. The division says on every occasion, and prints on every report, that the result is semi-quantitative and may be used for comparison only; it is not a figure for fineness that can be quoted as such.
- Ink and paper
- Colour, penetration and fluorescence distinguish iron-gall ink, carbon ink and modern ink; raking and transmitted light show the density of the laid lines, the direction in which the sheet was formed, and any repair. Since the fibre projector failed in 2019, the fibre composition of paper is measured for the Institute by a partner institution, and only visual and fluorescence observations are made here.
- Specific gravity and non-destructive testing
- Specific gravity is taken on the precision balance by weighing in air and in water, and is used as a check on the element analysis. Sampling from an original is never done. Where nothing else will answer the question, the applicant is advised to approach an institution equipped for it.
- Conservation: technical support and advice
- Advice is given on the choice of repair materials, pastes, lining papers and protective covers, and on the temperature and humidity appropriate to a store or a display case. Treatment itself is the business of the repair workshop; the division supplies the material science.
2. The instruments
The complete list of the laboratory's equipment is on the premises page, Table 2. Those the division uses daily, and their state, are these; the list is checked twice a year, in March and September.
| No. | Instrument | Acquired | State | Use in this division |
|---|---|---|---|---|
| L-01 | Precision balance, 0.01 mg | 2008 | in use | On the anti-vibration table in the inner room. Calibrated against standard weights before each session; the calibration is entered in the balance-room book. |
| L-02 | Portable X-ray fluorescence spectrometer | 2008, detector 2017 | in use | Sixty to one hundred and twenty seconds a measurement. Two people must be present and the instrument is never held in the hand; since the division has one member, it is used only when Dr Andersen or Mr Stein can attend, which in practice means about one session a fortnight. |
| L-03 | Stereomicroscope, 7× to 45× | 2008 | in use | Eyepiece graticule; grading of die wear and examination of paper fibre. |
| L-04 | Ultraviolet lamp, 365 nm | 2008 | in use | Exposure of an original never exceeds three minutes, and a mask confines the beam; the duration is entered in the record. |
| L-05 | Fibre projector | 1994 | out of action | The lamp ballast failed in 2019 and the part must be made to order by the maker. Fibre measurement is at present done by a partner institution. |
| L-09 | Portable digital microscope | 2016 | in use | For objects that cannot be moved; loan from the Institute is entered in the book by the head of division. Still in use, and now the division's chief means of examining anything at all. |
| L-10 | Temperature and humidity recorders, three | 2013 | in use | In the strongroom, the attic store and the library; read by hand twice a week and checked against the instrument record. |
About the fibre projector. The instrument has been out of use since 2019 and the maker has been asked twice for a price. The answer received in 2023 was that the ballast must be made as a single item and that the cost, with calibration, would come to about two years of the Institute's equipment budget; the conference therefore deferred it and arranged for fibre measurement to be done by a partner institution instead, which takes about six weeks a batch. Meanwhile every conclusion the division draws about paper carries the note "fibre composition not measured". The decision is in the minutes of 9 May 2023 (archive, Akt 26/4).
3. How testing is done
- Ask what the question is. An application must say what is to be decided — whether two coins come from the same mint, for instance — so that the method and the number of measurements can be chosen. Where no question has been formulated, the division formulates one with the applicant before starting.
- Nothing destructive. No sample is taken, nothing is scraped and nothing is burnt. Where that is the only way, the applicant is advised to go elsewhere.
- The semi-quantitative warning is printed. On the first page of every X-ray fluorescence report, in the same size of type as the rest: the result is semi-quantitative and is for comparison only. It is never relegated to a footnote.
- Two people present. Work with L-02 or L-04 requires two people, one operating and one recording, and the record includes the date, the operator, the room conditions and the duration of exposure.
- Raw values first. Reports give the measured values before any converted figure, and state the standard used for the conversion and where it comes from.
- No attributions. A report says what was observed. It does not pronounce on authenticity, date or value; questions of date and attribution go to Division I or Division II and are answered by their procedures.
4. Work done for others
| Year | Applicant | Work | Use made of the result |
|---|---|---|---|
| 2022 | A museum in the Land | Semi-quantitative analysis of 240 coins | Labels for a display. The division gave comparisons only and no figure for fineness. |
| 2022 | Two partner archives | Fluorescence examination of the ink on thirty-six charters | Separating original ink from later additions, for the archives' pre-treatment record. |
| 2023 | A university project | Specific gravity of 180 coins | A table in the project's dissertation; the division required the semi-quantitative limitation to be stated in the text. |
| 2023 | A parish, through the church archive office | Paper and binding of twelve registers | To help the parish decide whether conservation was needed. |
| 2024 | Two museums in the Land | Arrangement and registration of coin collections, in batches | Under the agreement of 1985; the volume of work is settled batch by batch. |
| 2024 | Division I of this Institute | Fineness series of the Goslar mint, 480 coins | Data for project WI-2022-03. |
5. Projects and publications
| Reference | Subject | Direction | Stage |
|---|---|---|---|
| WI-2022-03 | Fineness series of the Goslar mint, 1520–1620 | T. Bruns, with Division I | Running. 480 measurements made; the series curve awaits checking. |
| WI-2020-04 | Review of the dates of undated charters | T. Bruns, with Division II | Running. 148 charters done; thirty-one ranges narrowed as a result. |
| WI-2023-25 | A calibration procedure for the portable instrument | T. Bruns and P. Schneider | Running. Nine rules drafted, covering the use of standard pieces and the form of the record; to be applied with every test from 2025. |
| WI-2024-26 | Advice on store and display conditions, collected | P. Schneider | From March 2024. Seventy-four answers given since 2015 brought together; to be printed in 2025. |
| WI-2024-27 | Ageing of conservation materials, with the repair workshop | T. Bruns and L. Vogel | From July 2024. Samples of covers made in 2012, to be watched for five years. |
| Year | Title | Author | Where published |
|---|---|---|---|
| 2011 | Semi-quantitative analysis of coin alloys: a note on method | T. Bruns | Mitteilungen no. 40, pp. 12–24 |
| 2017 | Fluorescence examination of ink: three cases and its limits | T. Bruns and B. Ahrendt | Series, vol. 31 |
| 2019 | The balance and the eye: using and misusing test results in dating | T. Bruns | Series, vol. 32 |
| 2021 | A scale of die wear and its use | M. Kaltenbrunner and T. Bruns | Series, vol. 33 |
| 2023 | Advice on store and display conditions, 2015–2022 | P. Schneider | Printed internally; obtainable on application |
| 2024 | Draft calibration rules | T. Bruns and P. Schneider | Mitteilungen no. 62, in the press |
6. Commissioning work
| Step | What happens |
|---|---|
| 1. Write first | By e-mail to labor [at] winddew.lab or by post, stating the kind of object, how many there are, what is to be decided and the date proposed. A reply follows within five working days, accepting the work or not and fixing a date. |
| 2. Send or bring in | Objects may be posted or brought. Write before posting, saying how they are packed and whether they are insured; anything sent without warning is not held at the Institute's risk. |
| 3. Testing | On the date arranged. The applicant may attend, but may not operate the instruments. |
| 4. The record | One test record is issued, further copies on request, stating method, conditions, raw values and the semi-quantitative limitation. No attribution is given. Routine work is ready within ten working days. |
| 5. Charges | Partner institutions and public museums, free. Other academic institutions, from €6.00 an item according to the method. No certificate other than the test record is issued. The director decides on remissions. |
Every test record is entered in Division V's index of test records (KI-10, at present 18,740 entries) and is subject to the ordinary closure periods: where the applicant is a private person, the name does not appear in any document supplied to others, and the record itself is kept for twenty years. Work is not accepted on condition that it be left out of the index.
Compiled by Division VI. Questions about commissioned testing, calibration or conservation materials should be put to the head of division, Dr Bruns, extension 51.
Page WI-ABT-06 · compiled by T. Bruns · edited by the academic office · last modified 18 September 2026
